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By Suk-Joong L. Kang, Rajendra Bordia, Eugene A. Olevsky, Didier Bouvard

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Mexico. , Mexico 4 Institute de Investigaciones Metalurgicas, Universidad Michoacana de San Nicolas de Hidalgo, Edif. U, CU, Apdo. P. , Mexico ABSTRACT The main objective of this work was to study various aspects during the production of S^Fei+xMoi-xOo samples with different x composition by solid-state reaction method. The synthesis consisted of three steps; ball milling, calcination, and reduction. 9%) were mixed using a high energy ball milled at 1800 rpm for 6 h. Then, 20 mg of powder were calcinated in dried air at 1100°C.

Svehla, Technical Report TR R-132, NASA, Lewis Research Center, Cleveland, Ohio, 1962. |3 Z. A. Munir, 'Analytical treatment of the role of surface oxide layers in the sintering of metals', J. Mater. , 14 2733-2740 (1979). Advances in Sintering Science and Technology II · 53 Advances in Sintering Science and 1 echnology 11 Edited by Suk-Joong L. Kang, Rajendra Bordia, Eugene Olevsky and Didier Bouvard Copyright © 2012 The American Ceramic Society Microstructural Evolution and Physical Properties Advances in Sintering Science and 1 echnology 11 Edited by Suk-Joong L.

Shaw, A. H. , 31 55-59 (1983). 3 H. J. Möller, G. Welsch, "Sintering of Ultrafine Silicon Powder', J. Am. Ceram. Soc, 68 320-325 (1985). ''W. M. Robertson, "Thermal Etching and Grain-Boundary Grooving of Silicon Ceramics', J. Am. Ceram. Soc, 64 9-13 (1981). 5 W. S. Coblenz, 'The Physics and Chemistry of the Sintering of Silicon', J. Maler. , 25 2754-2764 (1990). 52 · Advances in Sintering Science and Technology II Sintering of Silicon, Effect of the Sample Size on Silica Reduction Kinetics and Densification 6 Y.

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